All cells were cycled inside a temperature-controlled environmental chamber (BTZ-133, ESPEC Corp.) using a MACCOR Model 2200 battery tester. After sealing, the cells underwent formation cycles which consisted of a C/10 (10.1 mA) constant current charge to 4.4 V, followed by a CV hold at 4.4 V until a current of C/20 (5.05 mA) was attained.
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